TA Instruments

AR1756-0002f

15/03/2013 14:45:46

Sample name	ASW Blank coupon#20 + DI + beads 
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	2 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 14:45:46

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 100.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99600	76.83	677.36	10000	20.0	0.1546	0.996	220.8	96.04	2.299	629.9	60.1138	0.06829	75.142	7514.2	3.411E-3	0.0	0.0
1.9960	99.99	112.96	10000	20.0	0.1510	1.996	36.82	125.0	0.2946	615.0	192.2000	0.03937	240.25	24025	3.411E-3	0.0	0.0
2.9960	99.99	113.46	10000	20.0	0.1487	2.996	36.98	125.0	0.2959	605.9	279.9830	0.03878	349.98	34998	3.411E-3	0.0	0.0
3.9960	100.0	110.90	10000	20.0	0.1443	3.996	36.15	125.0	0.2892	587.7	367.9300	0.03762	459.91	45991	3.411E-3	0.1	0.1
5.0000	100.0	112.42	10000	20.0	0.1461	5.000	36.64	125.0	0.2931	595.2	456.7100	0.03809	570.89	57089	3.411E-3	0.1	0.1
5.9960	100.0	112.06	10000	20.0	0.1434	5.996	36.53	125.0	0.2922	584.4	587.8960	0.03740	734.87	73487	3.411E-3	0.1	0.1
6.9960	100.0	113.01	10000	20.0	0.1438	6.996	36.83	125.0	0.2947	586.1	675.7930	0.03751	844.74	84474	3.411E-3	0.1	0.1
7.9960	100.0	111.86	10000	20.0	0.1459	7.996	36.46	125.0	0.2917	594.4	763.8710	0.03804	954.84	95484	3.411E-3	0.1	0.1
9.0000	100.0	112.69	10000	20.0	0.1438	9.000	36.73	125.0	0.2939	586.1	896.0560	0.03751	1120.1	1.1201E5	3.411E-3	0.2	0.2
10.004	100.0	110.69	10000	20.0	0.1441	10.004	36.08	125.0	0.2886	586.9	983.6980	0.03756	1229.6	1.2296E5	3.411E-3	0.2	0.2
10.996	100.0	111.42	10000	20.0	0.1461	10.996	36.32	125.0	0.2905	595.2	1071.6600	0.03809	1339.6	1.3396E5	3.411E-3	0.2	0.2
11.996	100.0	110.49	10000	20.0	0.1465	11.996	36.01	125.0	0.2881	596.8	1159.5601	0.03820	1449.5	1.4495E5	3.411E-3	0.2	0.2
13.000	100.0	109.20	10000	20.0	0.1459	13.000	35.59	125.0	0.2847	594.4	1292.1200	0.03804	1615.2	1.6152E5	3.411E-3	0.2	0.2
13.996	100.0	108.77	10000	20.0	0.1485	13.996	35.45	125.0	0.2836	605.1	1379.4900	0.03873	1724.4	1.7244E5	3.411E-3	0.2	0.2
15.004	100.0	110.68	10000	20.0	0.1505	15.004	36.08	125.0	0.2886	613.4	1467.4200	0.03926	1834.3	1.8343E5	3.411E-3	0.3	0.3
15.996	100.0	110.71	10000	20.0	0.1414	15.996	36.09	125.0	0.2887	576.2	1556.4399	0.03688	1945.6	1.9456E5	3.411E-3	0.3	0.3
16.996	100.0	110.26	10000	20.0	0.1451	16.996	35.94	125.0	0.2875	591.1	1687.3700	0.03783	2109.2	2.1092E5	3.411E-3	0.3	0.3
17.996	100.0	110.43	10000	20.0	0.1441	17.996	35.99	125.0	0.2879	586.9	1775.9301	0.03756	2219.9	2.2199E5	3.411E-3	0.3	0.3
19.000	100.0	109.60	10000	20.0	0.1453	19.000	35.72	125.0	0.2858	591.9	1863.2600	0.03788	2329.1	2.3291E5	3.411E-3	0.3	0.3
20.004	100.0	110.47	10000	20.0	0.1424	20.004	36.01	125.0	0.2881	580.3	1995.2200	0.03714	2494.0	2.4940E5	3.411E-3	0.3	0.3
20.996	100.0	110.13	10000	20.0	0.1459	20.996	35.90	125.0	0.2872	594.4	2083.1499	0.03804	2603.9	2.6039E5	3.411E-3	0.3	0.3
22.000	100.0	110.05	10000	20.0	0.1469	22.000	35.87	125.0	0.2870	598.5	2171.1201	0.03830	2713.9	2.7139E5	3.411E-3	0.4	0.4
22.996	100.0	110.19	10000	20.0	0.1479	22.996	35.92	125.0	0.2873	602.6	2259.5500	0.03857	2824.4	2.8244E5	3.411E-3	0.4	0.4
23.996	100.0	110.29	10000	20.0	0.1461	23.996	35.95	125.0	0.2876	595.2	2391.0500	0.03809	2988.8	2.9888E5	3.411E-3	0.4	0.4
25.000	100.0	107.82	10000	20.0	0.1463	25.000	35.14	125.0	0.2812	596.0	2479.0801	0.03815	3098.9	3.0989E5	3.411E-3	0.4	0.4
25.996	100.0	108.39	10000	20.0	0.1473	25.996	35.33	125.0	0.2826	600.2	2567.7500	0.03841	3209.7	3.2097E5	3.411E-3	0.4	0.4
26.996	100.0	108.48	10000	20.0	0.1443	26.996	35.36	125.0	0.2829	587.7	2699.8101	0.03762	3374.8	3.3748E5	3.411E-3	0.4	0.4
27.996	100.0	108.42	10000	20.0	0.1455	27.996	35.34	125.0	0.2827	592.7	2786.9099	0.03793	3483.6	3.4836E5	3.411E-3	0.5	0.5
28.996	100.0	110.20	10000	20.0	0.1457	28.996	35.92	125.0	0.2874	593.5	2874.8601	0.03799	3593.6	3.5936E5	3.411E-3	0.5	0.5
30.000	100.0	110.13	10000	20.0	0.1438	30.000	35.90	125.0	0.2872	586.1	2962.8301	0.03751	3703.5	3.7035E5	3.411E-3	0.5	0.5
31.004	100.0	109.49	10000	20.0	0.1422	31.004	35.69	125.0	0.2855	579.5	3094.7600	0.03709	3868.5	3.8685E5	3.411E-3	0.5	0.5
31.992	100.0	108.97	10000	20.0	0.1430	31.992	35.52	125.0	0.2842	582.8	3182.7800	0.03730	3978.5	3.9785E5	3.411E-3	0.5	0.5
32.996	100.0	108.95	10000	20.0	0.1461	32.996	35.51	125.0	0.2841	595.2	3270.7100	0.03809	4088.4	4.0884E5	3.411E-3	0.5	0.5
33.996	100.0	109.35	10000	20.0	0.1441	33.996	35.64	125.0	0.2851	586.9	3358.6499	0.03756	4198.3	4.1983E5	3.411E-3	0.6	0.6
35.000	100.0	109.85	10000	20.0	0.1463	35.000	35.81	125.0	0.2865	596.0	3490.5400	0.03815	4363.2	4.3632E5	3.411E-3	0.6	0.6
35.996	100.0	109.68	10000	20.0	0.1459	35.996	35.75	125.0	0.2860	594.4	3578.9700	0.03804	4473.7	4.4737E5	3.411E-3	0.6	0.6
37.000	100.0	110.09	10000	20.0	0.1471	37.000	35.88	125.0	0.2871	599.3	3666.5100	0.03836	4583.1	4.5831E5	3.411E-3	0.6	0.6
37.996	100.0	109.36	10000	20.0	0.1465	37.996	35.64	125.0	0.2852	596.8	3754.4600	0.03820	4693.1	4.6931E5	3.411E-3	0.6	0.6
39.000	100.0	109.29	10000	20.0	0.1483	39.000	35.62	125.0	0.2850	604.3	3886.9600	0.03867	4858.7	4.8587E5	3.411E-3	0.7	0.7
39.996	100.0	109.37	10000	20.0	0.1441	39.996	35.65	125.0	0.2852	586.9	3974.3701	0.03756	4968.0	4.9680E5	3.411E-3	0.7	0.7
40.996	100.0	109.12	10000	20.0	0.1445	40.996	35.57	125.0	0.2845	588.6	4062.3701	0.03767	5078.0	5.0780E5	3.411E-3	0.7	0.7
41.996	100.0	108.69	10000	20.0	0.1441	41.996	35.43	125.0	0.2834	586.9	4194.3301	0.03756	5242.9	5.2429E5	3.411E-3	0.7	0.7
42.996	100.0	108.33	10000	20.0	0.1469	42.996	35.31	125.0	0.2825	598.5	4283.1899	0.03830	5354.0	5.3540E5	3.411E-3	0.7	0.7
43.996	100.0	108.18	10000	20.0	0.1455	43.996	35.26	125.0	0.2821	592.7	4370.2700	0.03793	5462.8	5.4628E5	3.411E-3	0.7	0.7
45.000	100.0	108.20	10000	20.0	0.1465	45.000	35.27	125.0	0.2822	596.8	4458.1602	0.03820	5572.7	5.5727E5	3.411E-3	0.8	0.8
45.996	100.0	108.69	10000	20.0	0.1471	45.996	35.43	125.0	0.2834	599.3	4590.0698	0.03836	5737.6	5.7376E5	3.411E-3	0.8	0.8
46.996	100.0	109.02	10000	20.0	0.1461	46.996	35.53	125.0	0.2843	595.2	4681.2700	0.03809	5851.6	5.8516E5	3.411E-3	0.8	0.8
47.996	100.0	109.59	10000	20.0	0.1461	47.996	35.72	125.0	0.2858	595.2	4766.0298	0.03809	5957.5	5.9575E5	3.411E-3	0.8	0.8
48.996	100.0	110.07	10000	20.0	0.1469	48.996	35.88	125.0	0.2870	598.5	4898.6699	0.03830	6123.3	6.1233E5	3.411E-3	0.8	0.8
50.000	100.0	111.93	10000	20.0	0.1418	50.000	36.48	125.0	0.2919	577.8	4985.9302	0.03698	6232.4	6.2324E5	3.411E-3	0.8	0.8
50.996	100.0	109.42	10000	20.0	0.1487	50.996	35.67	125.0	0.2853	605.9	5073.8999	0.03878	6342.4	6.3424E5	3.411E-3	0.8	0.8
51.996	100.0	110.19	10000	20.0	0.1455	51.996	35.92	125.0	0.2873	592.7	5161.8398	0.03793	6452.3	6.4523E5	3.411E-3	0.9	0.9
52.992	100.0	108.52	10000	20.0	0.1465	52.992	35.37	125.0	0.2830	596.8	5293.7700	0.03820	6617.2	6.6172E5	3.411E-3	0.9	0.9
53.996	100.0	109.59	10000	20.0	0.1438	53.996	35.72	125.0	0.2857	586.1	5381.7598	0.03751	6727.2	6.7272E5	3.411E-3	0.9	0.9
55.004	100.0	108.68	10000	20.0	0.1491	55.004	35.42	125.0	0.2834	607.6	5469.7300	0.03888	6837.2	6.8372E5	3.411E-3	0.9	0.9
55.996	100.0	109.02	10000	20.0	0.1449	55.996	35.53	125.0	0.2843	590.2	5557.7002	0.03778	6947.1	6.9471E5	3.411E-3	0.9	0.9
56.996	100.0	108.33	10000	20.0	0.1477	56.996	35.31	125.0	0.2825	601.8	5689.6099	0.03852	7112.0	7.1120E5	3.411E-3	0.9	0.9
57.996	100.0	109.88	10000	20.0	0.1455	57.996	35.81	125.0	0.2865	592.7	5777.6099	0.03793	7222.0	7.2220E5	3.411E-3	1.0	1.0
58.996	100.0	108.46	10000	20.0	0.1445	58.996	35.35	125.0	0.2828	588.6	5866.1099	0.03767	7332.6	7.3326E5	3.411E-3	1.0	1.0
60.004	100.0	109.98	10000	20.0	0.1187	60.004	35.85	125.0	0.2868	483.6	5998.1001	0.03095	7497.6	7.4976E5	3.411E-3	1.0	1.0

